The development of a novel APGD plasma reactor equipped with an ultrasonic nozzle enabled the creation of thick coatings from cyclotetrasiloxane monomers. Control of the feed gas allowed the rapid deposition of both hydrophobic polysiloxane like films and hydrophilic SiOx gas barrier coatings. The APGD deposition methodology was extended to the creation of organic plasma polymers.
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A six membered decalactone ( DL) was also used for the synthesis of a diblock copolymer (mPEG b PDL) to compare the reaction kinetics and properties of the copolymers. The copolymers were prepared via bulk polymerisation using 1,5,7 Triazabicyclo[4.4.0]dec 5 ene (TBD) as a metal free catalyst to replace the conventionally used stannous octoate [Sn(Oct)2]. A higher polymerization efficiency was achived with TBD compared to Sn(Oct)2 catalyst.
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Tests show that for a finite element grid to model elastic wave propagation it is essential for there to be at least eight elements per wavelength. If this requirement is violated the predicted stresses are seriously affected, and the results of previously published studies must be judged against this condition. The model grid is designed to meet this requirement for the propagation velocity typical of dam materials and the frequencies typical of seismic events.
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